Crystal structure of bis{[(cyclohexylimino)(phenylimino)-l5-(methyl)diethylazane-κ 2 N:N′]-(ethyl)-zinc(II)]}, C38H62N6Zn2

Author:

Han Hong-Fei12ORCID,Li Hao-Yang1,Wang Song1,Wei Xue-Hong2

Affiliation:

1. College of Chemistry and Materials , Taiyuan Normal University , Jinzhong , Shanxi 030619 , China

2. School of Chemistry and Chemical Engineering , Shanxi University , Taiyuan , Shanxi 030006 , China

Abstract

Abstract C38H62N6Zn2, triclinic, P 1 $P\overline{1}$ (no. 2), a = 9.5907(4) Å, b = 10.6743(4) Å, c = 11.2593(4) Å, α =  107.6980 ( 10 ) $107.6980{(10)}^{\circ }$ , β =  113.5840 ( 10 ) $113.5840{(10)}^{\circ }$ , γ =  97.2290 ( 10 ) $97.2290{(10)}^{\circ }$ , V = 965.12(6) Å3, Z = 1, R gt(F) = 0.0232, wR ref(F 2) = 0.0577, T = 200(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Reference18 articles.

1. Sheldrick, G. M. Crystal structure refinement with Shelxl. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.

2. Bruker. Sadabs; Bruker AXS Inc.: Madison, WI, USA, 2000.

3. Bruker. Apex3 and Saint; Bruker AXS Inc.: Madison, WI, USA, 2016.

4. Brandenburg, K. Diamond. Visual Crystal Structure Information System. Version 4.2.2; Crystal Impact: Bonn, Germany, 2016.

5. Ali, A. R., Ghosh, H., Patel, B. K. A greener synthetic protocol for the preparation of carbodiimide. Tetrahedron Lett. 2010, 51, 1019–1021; https://doi.org/10.1016/j.tetlet.2009.12.017.

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