Affiliation:
1. Department of Chemistry , Ibaraki University , Mito , Ibaraki , 310-8512, Japan
2. Research Centre for Crystalline Materials, School of Science and Technology, Sunway University , Bandar Sunway , 47500, Selangor Darul Ehsan , Malaysia
Abstract
Abstract
C30H28BClCuN6, triclinic,
P
1
‾
$P‾{1}$
(no. 2), a = 11.549(3) Å, b = 12.321(3) Å, c = 12.348(4) Å, α = 111.785(1)°, β = 116.664(3)°, γ = 97.513(1)°, V = 1361.3(7) Å3, Z = 2, R
gt
(F) = 0.0440, wR
ref
(F
2) = 0.1063, T = 197 K.
Subject
Inorganic Chemistry,Condensed Matter Physics,General Materials Science
Reference23 articles.
1. REQAB; Rigaku Corporation: Tokyo, Japan, 1998.
2. CrystalClear. SMExpert; Rigaku Corporation: Tokyo, Japan, 2019.
3. Burla, M. C., Caliandro, R., Carrozzini, B., Cascarano, G. L., Cuocci, C., Giacovazzo, C., Mallamo, M., Mazzone, A., Polidori, G. Crystal structure determination and refinement via SIR2014. J. Appl. Crystallogr. 2015, 48, 306–309; https://doi.org/10.1107/s1600576715001132.
4. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.
5. Farrugia, L. J. WinGX and ORTEP for windows: an update. J. Appl. Crystallogr. 2012, 45, 849–854; https://doi.org/10.1107/s0021889812029111.