Crystal structure of 4-bromo-2-(4-chlorophenyl)-1-methyl-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile, C13H7BrClF3N2-Reference-Cited by-同舟云学术

Crystal structure of 4-bromo-2-(4-chlorophenyl)-1-methyl-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile, C₁₃H₇BrClF₃N₂

Published:2023-12-08 Issue:1 Volume:239 Page:131-132
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Qin Jia-Rui¹^ORCID,Tang Wen-Hao¹,Li Kai¹,Pan Hai-Yu¹

Affiliation:

1. School of Pharmacy, North China University of Science and Technology , 063210 Caofeidian District , Tangshan , P.R. China

Abstract

Abstract C13H7BrClF3N2, monoclinic, P21/c (no. 14), a = 9.4183(18) Å, b = 15.185(3) Å, c = 13.1826(18) Å, β = 133.905(8)°, V = 1358.4(4) Å3, Z = 4, R gt (F) = 0.0420, wR ref (F 2) = 0.1015, T = 293 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2023-0472/pdf

Reference11 articles.

1. Bruker. SAINT, APEX2 and SADABS; Bruker AXS Inc.: Madison, WI, USA, 2012.

2. Sheldrick, G. M. SHELXTL – integrated space-group and crystal-structure determination. Acta Crystallogr. 2015, A71, 3–8.

3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8, https://doi.org/10.1107/s2053229614024218.

4. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.

5. Grapov, A. F. Novel insecticides and acaricides. Russ. Chem. Rev. 1999, 68, 697–707; https://doi.org/10.1070/rc1999v068n08abeh000510.