Affiliation:
1. School of Basic Medical Science, Guizhou Medical University , Guiyang , 550025 , People’s Republic of China
Abstract
Abstract
C30H40N2NiO2, orthorhombic, Pnma (no. 62), a = 12.8114(19) Å, b = 21.301(3) Å, c = 10.6536(16) Å, V = 2907.3(8) Å3, Z = 4, R
gt(F) = 0.0290, wR
ref(F
2) = 0.0808, T = 273(2) K.
Subject
Inorganic Chemistry,Condensed Matter Physics,General Materials Science
Reference12 articles.
1. Sheldrick, G. M. Program SADABS: Area-Detector Absorption Correction; University of Göttingen: Germany, 1996.
2. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8; https://doi.org/10.1107/s2053229614024218.
3. Dolomanov, O. V., Bourhis, L. J., Gildea, R. J., Howard, J. A. K., Puschmann, H. OLEX2: a complete structure solution, refinement and analysis program. J. Appl. Crystallogr. 2009, 42, 339–341; https://doi.org/10.1107/s0021889808042726.
4. Brandenburg, K. DIAMOND. Visual Crystal Structure Information System. Ver.0; Crystal Impact: Bonn, Germany, 2015.
5. Dong, Q., Yang, X.-J., Gong, S., Luo, Q., Li, Q.-S., Su, J.-H., Zhao, Y., Wu, B. Distinct stepwise reduction of a nickel–nickel-bonded compound containing an α-diimine ligand: from perpendicular to coaxial structures. Chem. Eur. J. 2013, 19, 15240–15247; https://doi.org/10.1002/chem.201302463.