Synthesis and crystal structure of poly[aqua(μ4-(1R,2S,4R)-4-hydroxy-1-((7-hydroxy-3-(4-hydroxy-3-sulfonatophenyl)-4-oxo-4H-chromen-8-yl)methyl)pyrrolidin-1-ium-2-carboxylate-κ4 O:O′:O″:O‴)sodium(I)] monohydrate, C21H22NNaO12S-Reference-Cited by-同舟云学术

Synthesis and crystal structure of poly[aqua(μ₄-(1R,2S,4R)-4-hydroxy-1-((7-hydroxy-3-(4-hydroxy-3-sulfonatophenyl)-4-oxo-4H-chromen-8-yl)methyl)pyrrolidin-1-ium-2-carboxylate-κ⁴ O:O′:O″:O‴)sodium(I)] monohydrate, C₂₁H₂₂NNaO₁₂S

Published:2022-06-08 Issue:4 Volume:237 Page:733-735
ISSN:1433-7266
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
language:en
Short-container-title:

Author:

Chen Hai-Lin¹^ORCID,Huang Xiu-Xiang¹,Lan Jian-Jing¹,Yao Dong-Mei¹,Wang Yan-Ping¹,Liu Qiu-Ping¹

Affiliation:

1. School of Chemical and Biological Engineering, Hechi University , Yizhou District , Hechi , Guangxi , 546300 , P. R. China

Abstract

Abstract C21H22NNaO12S, orthorhombic, P212121 (no. 19), a = 7.6850(1) Å, b = 10.8030(1) Å, c = 25.9262(2) Å, V = 2152.42(4) Å3, Z = 4, R gt(F) = 0.0309, wR ref(F 2) = 0.0818, T = 100.0(4) K.

Funder

the Foundation of Hechi University

Guangxi Natural Science Foundation of China

2021 High-level Talents Scientific Research Startup Fund of Hechi University

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/document/doi/10.1515/ncrs-2022-0208/pdf

Reference19 articles.

1. Rigaku. CrysAlisPro; Rigaku Corporation: Yarnton, Oxfordshire, England, 2020.

2. Brandenburg, K. Diamond. Visual Crystal Structure Information System. Ver. 3.2; Crystal Impact: Bonn, Germany, 2012.

3. Sheldrick, G. M. Crystal structure refinement with SHELXL. Acta Crystallogr. 2015, C71, 3–8, https://doi.org/10.1107/s2053229614024218.

4. Sheldrick, G. M. SHELXTL- integrated space-group andcrystal-structure determination. Acta Crystallogr. 2015, A71, 3–8, https://doi.org/10.1107/s2053273314026370.

5. Parsons, S., Flack, H. D., Wagner, T. Use of intensity quotients and differences in absolute structure refinement. Acta Crystallogr. 2013, B69, 249–259, https://doi.org/10.1107/s2052519213010014.