Crystal structure of 2-(4-ammoniocyclohexyl)-3-(pyridin-2-yl)imidazo[1,5-a]pyridin-2-ium 2-[(2-carboxylatophenyl)disulfanyl]benzoate dihydrate, [C18H22N4][C14H8O4S2] ⋅ 2H2O

Author:

Tan Sang Loon1,Tiekink Edward R.T.1

Affiliation:

1. Research Centre for Crystalline Materials, School of Science and Technology, Sunway University, 47500 Bandar Sunway, Selangor Darul Ehsan, Malaysia

Abstract

Abstract[C18H22N4][C14H8O4S2]⋅2H2O, orthorhombic, P212121 (no. 19), a = 9.7616(1) Å, b = 16.7411(2) Å, c = 18.6843(2) Å, V = 3053.39(6) Å3, Z = 4, Rgt(F) = 0.0265, wRref(F2) = 0.0679, T = 100(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Reference18 articles.

1. A 1:2 co-crystal of 2,2′-thiodibenzoic acid and triphenylphosphane oxide: crystal structure, Hirshfeld surface analysis and computational study;Acta Crystallogr,2018

2. Crystal structure of the co-crystal 2-[(2-carboxyphenyl)disulfanyl]benzoic acid−3-chlorobenzoic acid (2/1), C35H25ClO10S4 Z;Kristallogr. NCS,2019

3. A short history of SHELX;Acta Crystallogr,2008

4. A short history of SHELX;Acta Crystallogr,2008

5. The importance of C—H⋯N, C-H⋯π and π⋯π interactions in the crystal packing of the isomeric N1,N4-bis((pyridine-n-yl)methylene)cyclohexane-1,4-diamines, n = 2, 3 and 4;CrystEngComm,2006

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