Crystal structure of {5,5′-((propane-1,3-diylbis(azanylylidene))bis(methanylylidene))bis(3-(ethoxycarbonyl)-2,4-dimethylpyrrol-1-ido)-κ4N,N′,N′′,N′′′}zinc(II), C23H30N4O4Cu

Author:

Han Xue-Feng1,Yang Qing-Wen2,Yang Miao2,Wu Wei-Na2

Affiliation:

1. Personnel Services, Henan Polytechnic University, Jiaozuo 454000, P.R. China

2. College of Chemistry and Chemical Engineering, Henan Polytechnic University, Jiaozuo 454000, P.R. China

Abstract

AbstractC13H17N3OS, monoclinic, P1̅ (no. 2), a = 7.746(6) Å, b = 12.344(9) Å, c = 12.655(9) Å, α = 95.766(7)°, β = 98.007(7)°, γ = 101.595(13)°, V = 1163.4(15) Å3, Z = 2, Rgt(F) = 0.0550, wRref(F2) = 0.1616, T = 296(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Reference12 articles.

1. Ni(II)/Cu(II)/Zn(II) complexes baded on a bis(pyrrol-2-yl-methyleneamine) ligand: syntheses, characterization, fluorescence properties and crystal structures of Ni(II)/Cu(II) complexes;Chin. J. Inorg. Chem,2016

2. Double-stranded helicates, triangles, and squares formed by the self-assembly of pyrrol-2-ylmethyleneamines and ZnII Ions;Angew. Chem. Int. Ed,2003

3. Self-assembly of bis(pyrrol-2-ylmethyleneamine) ligands with Cu(II) controlled by bridging [-(CH2)n-] spacers and weak intermolecular C—H⋯Cu hydrogen bonding;Eur. J. Inorg. Chem,2004

4. Synthesis, characterization, and antioxidant activities of three Cu(II) complexes with Schiff-base ligands;J. Coord. Chem,2010

5. Crystal refinement with SHELX;Acta Crystallogr,2015

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