Crystal structure of the (E)-O-methyl-N-phenyl-thiocarbamate – 4,4′-bipyridine (1/1), C18H17N3OS

Author:

Yeo Chien Ing1,Tiekink Edward R.T.1

Affiliation:

1. Research Centre for Crystalline Materials, School of Science and Technology, Sunway University, 47500 Bandar Sunway, Selangor Darul Ehsan, Malaysia

Abstract

AbstractC18H17N3OS, monoclinic, C2/c (no. 15), a = 13.4754(3) Å, b = 13.8997(3) Å, c = 18.0300(4) Å, β = 107.202(3)°, V = 3226.03(13) Å3, Z = 8, Rgt(F) = 0.0341, wRref(F2) = 0.0878, T = 100(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Reference20 articles.

1. Asymmetric bromolactonization using amino-thiocarbamate catalyst;J. Am. Chem. Soc,2010

2. A short history of SHELX;Acta Crystallogr,2008

3. Crystal structure of the bis((E)-O-ethyl-N-phenylthiocarbamate) – 4,4′-bipyridine co-crystal (2/1), C28H30N4O2S2;Z. Kristallogr. – NCS,2018

4. Asymmetric bromolactonization using amino-thiocarbamate catalyst;J. Am. Chem. Soc,2010

5. Prevalence of the thioamide {⋯H–N–C=S}2 synthon–solid-state (X-ray crystallography), solution (NMR) and gas-phase (theoretical) structures of O-methyl-N-aryl-thiocarbamides;CrystEngComm,2005

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