Crystal structure of bis[(2-(2-bromophenyl)-5-ethyl-1,3-dioxane-5-carboxylato-κO)-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ4N,N′,N′′,N′′′)]nickel(II) hemihydrate C42H65Br2N4NiO8.5
Author:
Qiong Wang1,
Jia Guo-Kai1,
Liu Xiao-Wen1
Affiliation:
1. Department of Biology and Chemistry, Hunan University of Science and Engineering, Yongzhou, Hunan 425199, P.R. China
Abstract
AbstractC42H65Br2N4NiO8.5, monoclinic, P21/c (no. 14), a = 14.852(2) Å, b = 12.1965(18) Å, c = 14.166(2) Å, β = 117.755(1)°, V = 2270.8(6) Å3, Z = 2, Rgt(F) = 0.0449, wRref(F2) = 0.1276, T = 296(2) K.
Publisher
Walter de Gruyter GmbH
Subject
Inorganic Chemistry,Condensed Matter Physics,General Materials Science
Reference14 articles.
1. Preparation and properties of bis(sodium sulfate) types of cleavable surfactants derived from diethyl tartrate;J. Oleo. Sci,2005
2. Crystal structure refinement with SHELXL;Acta Crystallogr,2015
3. Crystal structure of (4-(4-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylato)-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane)nickel(II) perchlorate monohydrate, C29H52Cl2N4NiO9;Z. Kristallogr. NCS,2018
4. SHELXT – integrated space-group and crystal-structure determination;Acta Crystallogr,2015