The synthesis and crystal structure of 5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazole-3-carboxamide–tetrahydrofuran (1/1), C16H14N4Cl2F6O3S

Author:

Chen Lianqing1,Yang Gengtao2,Wu Zhongda2

Affiliation:

1. Key Laboratory of Catalysis and Energy Materials Chemistry of Ministry of Education and Hubei Key Laboratory of Catalysis and Materials Science, South-Central University for Nationalities, Wuhan 430074, P.R.China, e-mail: chen_lianqing@163.com

2. Key Laboratory of Catalysis and Energy Materials Chemistry of Ministry of Education & Hubei Key Laboratory of Catalysis and Materials Science, South-Central University for Nationalities, Wuhan 430074, P.R. China

Abstract

AbstractC16H14N4Cl2F6O3S, monoclinic, P21/c (no. 14), a = 10.927(3) Å, b = 13.542(3) Å, c = 15.744(4) Å, β = 107.360(4)°, V = 2223.6(10) Å3, Z = 4, Rgt(F) = 0.0480, wRref(F2) = 0.1471, T = 294.15 K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Reference16 articles.

1. SHELXT – integrated space-group and crystal-structure determination;Acta Crystallogr,2015

2. Syntheses, structures and luminescent properties of two 3D pillared open frameworks with unique 6-connected structures based on 4,5-dihydroxy-1,3-benzenedisulfonate;J. Coord. Chem,2017

3. SHELXT – integrated space-group and crystal-structure determination;Acta Crystallogr,2015

4. Crystal structure of the fluorescent fipronil derivative 5,5′-(methylenebis(azanediyl))bis(1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazole-3-carbonitrile), C25H6N8O2Cl4F12S2;Z. Kristallogr. NCS,2019

5. Crystal structure of the fluorescent fipronil derivative 5,5′-(methylenebis(azanediyl))bis(1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazole-3-carbonitrile), C25H6N8O2Cl4F12S2;Z. Kristallogr. NCS,2019

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