Synthesis and crystal structure of bis(2-(((4-(1-(ethoxyimino)ethyl)phenyl)imino)methyl)-5-fluorophenolato-κ2N,O)zinc(II) - methanol (1/1), C33H32F2N4O4Zn

Author:

Zhao Ji-Xing1

Affiliation:

1. Analysis and Testing Center, Shihezi University, Xinjiang 832003, P.R. China

Abstract

AbstractC33H32F2N4O5Zn, triclinic, P1̄ (no. 2), a = 9.5132(5) Å, b = 13.0781(6) Å, c = 14.0448(6) Å, α = 63.0950(10)°, β = 73.5640(10)°, γ = 78.870(2)°, V = 1490.24(12) Å3, Z = 2, Rgt(F) = 0.0459, wRref(F2) = 0.1004, T = 173(2) K.

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Reference30 articles.

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2. OLEX2: a complete structure solution, refinement and analysis program;J. Appl. Crystallogr,2009

3. Crystal structure of bis{5-methoxy-2-((E)-((4-((E)-1-(methoxyimino)ethyl)phenyl)imino)methyl)phenolato-κ2N,O)}copper(II), C34H34CuN4O6;Z. Kristallogr. NCS,2017

4. Four 3d-4f heteromultinuclear zinc(II)-lanthanide(III) complexes constructed from a distinct hexadentate N2O2-type ligand: syntheses, structures and luminescence properties;J. Coord. Chem,2017

5. A short history of SHELX;Acta Crystallogr,2008

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