Crystal structure of cyclo[tetra(μ2-cyanido)-tetracyanido-bis(1,4,7,10-tetraazacyclododecane-κ4N,N′,N′′,N′′′)dinickel(II)dipalladium(II)] hexahydrate, C24H52N16Ni2O6Pd2-Reference-Cited by-同舟云学术

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Crystal structure of cyclo[tetra(μ2-cyanido)-tetracyanido-bis(1,4,7,10-tetraazacyclododecane-κ4N,N′,N′′,N′′′)dinickel(II)dipalladium(II)] hexahydrate, C24H52N16Ni2O6Pd2

Published:2019-12-18 Issue:1 Volume:235 Page:201-202
ISSN:2197-4578
Container-title:Zeitschrift für Kristallographie - New Crystal Structures
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Author:

Ha Kwang¹

Affiliation:

1. Chonnam National University, School of Chemical Engineering, Research Institute of Catalysis, Gwangju 61186, Republic of Korea

Abstract

AbstractC24H52N16Ni2O6Pd2, monoclinic, P21/c (no. 14), a = 8.6416(3) Å, b = 14.2237(5) Å, c = 15.5573(5) Å, β = 93.8054(12)°, V = 1908.02(11) Å3, Z = 2, Rgt(F) = 0.0312, wRref(F2) = 0.0915, T = 223(2) K.

Funder

Chonnam National University

Publisher

Walter de Gruyter GmbH

Subject

Inorganic Chemistry,Condensed Matter Physics,General Materials Science

Link

https://www.degruyter.com/downloadpdf/journals/ncrs/235/1/article-p201.xml

Reference8 articles.

1. ORTEP-3 for Windows-a version of ORTEP-III with a graphical user interface (GUI);J. Appl. Crystallogr,1997

2. Crystal structure refinement with SHELXL;Acta Crystallogr,2015

3. Cyano-bridged molecular squares: synthesis and structures of [Ni(cyclen)]2[Pt(CN)4]2⋅6H2O, [Ni(cyclen)]2[Ni(CN)4]2⋅6H2O and [Mn(cyclen)]2[Ni(CN)4]2⋅6H2O;Polyhedron,2006

4. Single-crystal structure validation with the program PLATON;J. Appl. Crystallogr,2003

5. Cyano-bridged molecular squares: synthesis and structures of [Ni(cyclen)]2[Pt(CN)4]2⋅6H2O, [Ni(cyclen)]2[Ni(CN)4]2⋅6H2O and [Mn(cyclen)]2[Ni(CN)4]2⋅6H2O;Polyhedron,2006

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