NaLiS: Ein weiteres Interalkalimetallsulfid / NaLiS: A nother Inter Alkaline Metal Sulphide-Reference-Cited by-同舟云学术

NaLiS: Ein weiteres Interalkalimetallsulfid / NaLiS: A nother Inter Alkaline Metal Sulphide

Published:1985-12-01 Issue:12 Volume:40 Page:1759-1760
ISSN:1865-7117
Container-title:Zeitschrift für Naturforschung B
language:en
Short-container-title:

Author:

Sabrowsky Horst¹,Thimm Alfred¹,Vogt-Mertens Petra¹

Affiliation:

1. Lehrstuhl für Anorganische Chem ie I (Arbeitsgruppe Festkörperchem ie), Ruhr-Universität Bochum , Universitätsstraße 150, D-4630 Bochum 1

Abstract

Abstract The colourless com pound NaLiS has been prepared and its structure determined by single crystal X-ray diffraction techniques. The very hygroscopic NaLiS crystallizes in the tetragonal space group P4/nmm (Z = 2) with the cell parameters a = 402.6(1), c = 649.5(2) pm. The structure was solved from 720 counter reflections (216 symmetry independent reflections) by differential Fourier syntheses. Refining gives a least squares residue of 0.024. The anti-PbFCl-type structure is characterized by layers of LiS4/4-tetrahedra connected by their edges in two dimensions and 2 interspersed layers of sodium

Publisher

Walter de Gruyter GmbH

Subject

General Chemistry

Link

https://www.degruyter.com/document/doi/10.1515/znb-1985-1229/pdf

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