Affiliation:
1. Institut für Anorganische Chemie der Universität Tübingen, Auf der Morgenstelle 18, D-7400 Tübingen
Abstract
Abstract
Novel trialkylstannanedithiocarboxylato complexes are formed in a one-pot reaction of R3SnCS2Li (R = benzyl, methyl, cyclohexyl) with BrM(CO)5 (M = Mn, Re) in a THF/dioxane solution. Tetracarbonylmetal species could be detected by IR spectroscopy in all cases. The more stable rhenium chelate complexes, R3SnCS2Re(CO)4, were isolated by chromatographic separation as yellow, low-melting solids with 10-20% yield.
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4 articles.
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