Preparation and characterization of AKD sizing agent by “one-pot cooking”

Author:

Huang Lian Qing1,Song Xiao Ming1,Cui Lu Qing1,Gao Shan Shan12,Chen Fu Shan1,Wang Song Lin1,Liu Jing Lin1

Affiliation:

1. Qingdao University of Science and Technology , No. 53 Zhengzhou Road , Qingdao City , Shandong Province , China

2. Department of Pulp and Paper Science and Technology , Ministry of Education , Qilu University of Technology / Key Laboratory of Shandong Province Qilu University of Technology , Jinan 250353 , China

Abstract

Abstract Alkyl ketone dimer (AKD) is a reactive sizing agent commonly used in neutral or alkaline papermaking. Most traditional methods consist in preparing the AKD emulsion and then adding it to a starch solution. In this study, the preparation process of the AKD sizing liquid was improved and optimized. A novel preparation method of the AKD sizing agent was proposed. The effects of different reaction parameters, such as temperature, time, stirring speed, emulsifier dosage and solid content were investigated. The optimum conditions for preparing the AKD sizing agent were determined, and the sizing liquid was characterized. It was found that the water resistance of the coated paper was the highest when the reaction was carried out at 75 °C for 20 min, at a stirring speed of 700 r/min, with the emulsifier dosage of 9 % and solids content of 15 %.

Funder

National Natural Science Foundation of China

Department of Education of Shandong Province

Shandong Province

Natural Science Foundation of Shandong Province

South China University of Technology

China Postdoctoral Science Foundation

Publisher

Walter de Gruyter GmbH

Subject

General Materials Science,Forestry

Reference29 articles.

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2. Cai, Q. H. (2011) A new type of liquid AKD surface sizing agent. International Papermaking 01:45–46.

3. Chen, F. S., Shang, X. L., Song, X. M. (2013) Synthesis and application of polydiallyldimethylammonium chloride [J]. Paper Science and Technology 1(2):45–49.

4. Dai, H. Q., Zheng, T. (1999) Preparation of AKD_LT neutral alkaline papermaking sizing agent. J. Nanjing Forestry University 23(01):33–37.

5. Fei, G. Q., Shen, Y. D., Wang, H. H. and Gong, B. H. (2008) Preparation and mechanism of macromolecule based AKD emulsion. China Papermaking 06:30–33.

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