Experimental and theoretical approaches on thermal and structural properties of Zn doped BSCCO glass ceramics-Reference-Cited by-同舟云学术

Experimental and theoretical approaches on thermal and structural properties of Zn doped BSCCO glass ceramics

Published:2016-03-01 Issue:1 Volume:34 Page:25-32
ISSN:2083-134X
Container-title:Materials Science-Poland
language:en
Short-container-title:

Author:

Koralay H.¹,Hicyilmaz O.¹,Cavdar S.¹,Ozturk O.²³,Tasci A.T.²

Affiliation:

1. Superconductivity and Thermal Analysis Laboratory, Department of Physics, Faculty of Sciences, Gazi University, 06531 Ankara, Turkey

2. Department of Physics, Faculty of Arts and Sciences, Kastamonu University, 37100 Kastamonu, Turkey

3. Research and Application Center, Kastamonu University, 37100 Kastamonu, Turkey

Abstract

Abstract Thermal properties of Cu–Zn partially substituted Bi1.8Sr2Ca2Cu3.2-xZnxO10+δ (x = 0, 0.1 and 0.5) glass-ceramic systems have been investigated with the help of a differential thermal analyzer (DTA) by using Johnson-Mehl-Avrami-Kolmogorov (JMAK) approximation. Non-isothermal crystallization kinetics of the samples has been tested. The calculated values of activation energy of crystallization (E) and Avrami parameter (n) ranged between 306.1 and 338.3 kJ.mol-1 and 1.29 and 3.59, respectively. Crystallization kinetics was compared following the partial substitution, before and after Zn doping of the sample. In addition, by using a scanning electron microscope (SEM) and X-ray powder diffractometer (XRD), structural properties of Zn doped BSCCO glass-ceramic samples were determined. Surface morphology of the samples was studied by SEM measurements. Lattice parameters and volume of the samples were calculated from the XRD measurements.

Publisher

Walter de Gruyter GmbH

Subject

Mechanical Engineering,Mechanics of Materials,Condensed Matter Physics,General Materials Science

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