Synthesis and characterization of heterostructured nanoparticle for efficient photocatalytic performance for dye degradation

Author:

Iqbal Munawar1,Shar Ghulam A.2,Ibrahim Sobhy M.34,Iftikhar Shan1,Asif Muhammad1,Khan Muhammad I.5,Kusuma Heri S.6,Yaseen Muhammad7,Nazir Arif1

Affiliation:

1. Department of Chemistry , The University of Lahore , Lahore 53700 , Pakistan

2. Institute of Chemistry, Shah Abdul Latif University , Khairpur , Sindh 66020 , Pakistan

3. Department of Biochemistry , College of Science, King Saud University , P.O. Box: 2455 , Riyadh 11451 , Saudi Arabia

4. Department of Analytical Chemistry and Control , Hot Laboratories and Waste Management Center, Atomic Energy Authority , Cairo 13759 , Egypt

5. Department of Physics , The University of Lahore , Lahore 53700 , Pakistan

6. Analytical Chemistry Research Group, Department of Chemical Education , Faculty of Education and Teachers Training, University of Nusa Cendana , Kupang , Nusa Tenggara Timur 85001 , Indonesia

7. Department of Physics , University of Agriculture , Faisalabad 38000 , Pakistan

Abstract

Abstract This paper focusses on the synthesis of cobalt vanadate (CoVO4) nanoparticles (NPs) by precipitation method. This was further augmented by assistance from microwave. Nanotechnology has been a wonderful tool with the promising application in different fields of life. The CoVO4 NPs synthesized by microwave assisted precipitation method was characterized by advanced techniques such as X-ray powder diffraction (XRD), Energy dispersive X-ray analysis (EDX), Scanning electron microscopy (SEM), Ultraviolet visible spectroscopy (UV–vis) techniques. Rhodamine B (RhB) dye was used to evaluate the photo catalytic activity (PCA) of NPs by degradation of dye. The conditions were optimized for maximum degradation of dye. The NPs were in the nano flowers form and the size was ≤100 nm. The results regarding degradation of RhB was through PCA were promising; 83% dye was degraded at pH 10, reaction time 160 min and catalyst dose 1 g. It may conclude that the synthesized NPs could further be employed for possible treatment of industrial effluents particularly textile industry.

Publisher

Walter de Gruyter GmbH

Subject

Physical and Theoretical Chemistry

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