1. a Chemistry Department , University of Southampton , Highfield, Southampton , S09 5NH , UK
2. b Department of Pure and Applied Chemistry , University of Strathclyde , Glasgow , G1 IXL , UK
3. e SERC Daresbury Laboratory , Warrington , WA4 4JD , UK
4. c Department of Physics , University of Warwick , Coventry , CV4 7AL , UK
5. d Applied Electrochemistry Group, Chemistry Department , Portsmouth Polytechnic , White Swan Road, Portsmouth , PO1 2DT , UK