1. a Physique des Milieux Condensés and Département Haute Pressions , Université P. et M. Curie, T. 13, Et. 4, B. 77, 4 place Jussieu , 75252, Paris , Cedex 05 , France
2. b Dept. of Physics , University of Edinburgh, Mayfield Road, Edinburgh , EH9, 352 , U.K.
3. c The ISIS Facility, Rutherford Appleton Laboratory , Didcot, Oxon, U.K.
4. d Dept. of Crystallography , Birkbeck College , London , WC1E 7HX , U.K.