1. a Department of Chemistry , Aarhus University , DK-8000, Arhus C , Denmark
2. b Institut Max von Laue-Paul Langevin , B.P. 156x, Centre de Tri, F-38042 , Grenoble Cédex , France
3. c Department of Physics , University of Helsinki , Siltavuorenpenger 20 D, SF-00170, Helsinki , 17 , Finland