1. a Institut Laue Langevin , 156X cedex, Grenoble, 38042, France
2. b Lab. L. Néel, CNRS/UJF , B. P. 166 cedex, Grenoble, 38042, France
3. c Lab. L. Néel, CNRS/UJF , B.P. 166, cedex, Grenoble, 38042, France
4. d Dept. of Physics , University of Warwick , Coventry, CV4 7AL, U.K.