Conformational Studies of 1-(2′-Hydroxythiobenzoyl)piperidine and 4-(2′-Hydroxythiobenzoyl)morpholine by High Resolution N.M.R. Spectroscopy-Reference-Cited by-同舟云学术

Conformational Studies of 1-(2′-Hydroxythiobenzoyl)piperidine and 4-(2′-Hydroxythiobenzoyl)morpholine by High Resolution N.M.R. Spectroscopy

Published:1975-01 Issue:2-3 Volume:8 Page:141-149
ISSN:0038-7010
Container-title:Spectroscopy Letters
language:en
Short-container-title:Spectroscopy Letters

Author:

Krueger Peter J.¹²,Fulea Adrian O.¹²³

Affiliation:

1. a Department of Chemistry , University of Calgary , Calgary , Alberta , Canada , T2N 1N4

2. b Cornelia Fulea and Felicia Cornea, Faculty of Chemistry , University of Bucharest , Bucharest , Romania

3. c Isaak Walton Killam Memorial Scholar; on leave o f absence from the University o f Bucharest

Publisher

Informa UK Limited

Subject

Spectroscopy,Atomic and Molecular Physics, and Optics,Analytical Chemistry

Link

https://www.tandfonline.com/doi/pdf/10.1080/00387017508067315

Reference15 articles.

1. This work was supported by the National Research Council of Canada. High resolution n.m.r. spectra were obtained at the Canadian 220 MHz N.M.R. Centre, Sheridan Park, Ontario. We are indebted to Prof. M. Anteunis, State University of Gent, Belgium, for some 300 MHz spectra. This work is part of the Ph.D. thesis of A. O. Fulea

2. I.r. spectra of dilute (c < 0.003 M) solutions in CCl4exhibit the following normal “free” νOH (trace only), νQH…S intramol. (broad and intense), and δνOH values: (la) 3605, 3255, 350; (2a) 3607, 3266, 341 cm−1. At this low concentration intermolecular association can be excluded. In the u.v. the n ν* transition in n-hexane solution shifts from 389 nm inlato 401 nm inlc, and from 389 nm2ato 403 nm in2c

3. Donor Properties of Some Sulfur Compounds

4. über die Struktur der Thioamide und ihrer Derivate, VI Zur magnetischen Anisotropie der Thioamid-Gruppe

5. The CS2 ? group as a conformational probe for cyclic amines: nuclear magnetic resonance study

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1. Critical comments and erratum: Intramolecular OH … S ⇌ O … HS proton transfer equilibrium in N-(o-hydroxythiobenzoyl)piperidines and -morpholines in acetone-d6 solution: i.r. and NMR studies;Spectrochimica Acta Part A: Molecular Spectroscopy;1986-01

2. On the chirality of 2-hydroxy-NN-dialkythiobenzamides. Demonstration of three consecutive conformational processes;J. Chem. Soc., Perkin Trans. 2;1980

3. Nuclear magnetic resonance spectra of o-hydroxythiobenzamides: the intramolecular hydrogen bond as a conformational probe;Canadian Journal of Chemistry;1977-01-15

4. Intramolecular OH ⋯ S α O ⋯ HS proton transfer equilibrium in N-(o-hydroxythiobenzoyl)piperidines and -morpholines in acetone-d6 solution: i.r. and n.m.r. studies;Spectrochimica Acta Part A: Molecular Spectroscopy;1977-01

5. 13C n.m.r. spectra of some thiobenzamides. Correlation between13C and1H n.m.r. spectra and signal assignments ofsyn andanti CH2 groups;Organic Magnetic Resonance;1976-10