A 13C-detected 15N double-quantum NMR experiment to probe arginine side-chain guanidinium 15Nη chemical shifts
Author:
Funder
Leverhulme Trust
Wellcome Trust
Publisher
Springer Science and Business Media LLC
Subject
Spectroscopy,Biochemistry
Link
http://link.springer.com/article/10.1007/s10858-017-0137-2/fulltext.html
Reference53 articles.
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2. André I, Linse S, Mulder FAA (2007) Residue-specific pKa determination of lysine and arginine side chains by indirect 15N and 13C NMR spectroscopy: application to apo calmodulin. J Am Chem Soc 129:15805–15813
3. Bax A, Freeman R, Frenkiel TA, Levitt MH (1981) Assignment of carbon-13 NMR spectra via double-quantum coherence. J Magn Reson 43:478–483
4. Bodenhausen G, Ruben DJ (1980) Natural abundance nitrogen-15 NMR by enhanced heteronuclear spectroscopy. Chem Phys Lett 69:185–189
5. Borders CL, Broadwater JA, Bekeny PA, Salmon JE, Lee AS, Eldridge AM, Pett VB (2008) A structural role for arginine in proteins: multiple hydrogen bonds to backbone carbonyl oxygens. Protein Sci 3:541–548
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