Development and Validation of a Multiresidue Method for the Determination of Macrocyclic Lactones, Monensin, and Fipronil in Bovine Liver by UHPLC-MS/MS Using a QuEChERS Extraction

Author:

Pastore Victor A. A.,Santos Flávio A.,Lana Mary Ane G.,Silva Guilherme R.,Figueiredo Tadeu C.,Assis Débora C. S.,Cançado Silvana V.ORCID

Funder

Conselho Nacional de Desenvolvimento Científico e Tecnológico

Publisher

Springer Science and Business Media LLC

Subject

Safety Research,Safety, Risk, Reliability and Quality,Applied Microbiology and Biotechnology,Food Science,Analytical Chemistry

Reference43 articles.

1. Barreto F, Ribeiro C, Hoff RB, Costa TD (2017) A simple and high-throughput method for determination and confirmation of 14 coccidiostats in poultry muscle and eggs using liquid chromatography - quadrupole linear ion trap - tandem mass spectrometry (HPLC-QqLIT-MS/MS): validation according to European Union 2002/657/EC. Talanta 168:43–51. https://doi.org/10.1016/j.talanta.2017.02.007

2. Brasil (2019) Normative Instruction 5 of april 23, 2019. Sampling plan and the reference limits for the National Plan for the Control of Residues and Contaminants in Animal Products - PNCRC of 2019, for the chains of beef, pork, goat, mutton, equine, rabbit, poultry, ostrich meat, and milk, fisheries, honey and eggs. Off Gaz Fed Gov. https://www.gov.br/agricultura/pt-br/assuntos/inspecao/produtos-animal/plano-de-nacional-de-controle-de-residuos-e-contaminantes/PNCRC2019SamplingPlan.pdf. Accessed June 10, 2021

3. Cid YP, Ferreira TP, Magalhães VS, Correia TR, Scott FB (2016) Injectable fipronil for cattle: plasma disposition and efficacy against Rhipicephalus microplus. Vet Parasitol 220:4–8. https://doi.org/10.1016/j.vetpar.2016.02.008

4. Codex Alimentarius (2018) Maximum residue limits (MRLs) and risk management recommendations (RMRs) for residues of veterinary drugs in foods. CX/MRL 2–2018. http://www.fao.org/fao-who-codexalimentarius/codex-texts/maximum-residue-limits/en/. Accessed 10 June 2021

5. Codex Alimentarius Commission (2014) Guidelines for the design and implementation of national regulatory food safety assurance programme associated with the use of veterinary drugs in food producing animals. CAC/GL 71–2009. 42p. http://www.fao.org/fao-who-codexalimentarius/codex-texts/guidelines/en/. Accessed 10 June 2021

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