Chlorine-atom abstraction and cluster fragmentation in the reaction of H3Re3(CO)10(MeCN)2 with the diphosphine ligand 4,5-bis(diphenylphosphino)-4-cyclopenten-1,3-dione (bpcd): X-ray diffraction structure of fac-ClRe(CO)3(bpcd)

Author:

Watson William H.,Kandala Srikanth,Richmond Michael G.

Publisher

Springer Science and Business Media LLC

Subject

Condensed Matter Physics,General Chemistry

Reference17 articles.

1. Wei, C.-Y.; Garlaschelli, L.; Bau, R.; Koetzle, T.F. J. Organomet. Chem. 1981, 213, 63. (b) Ciani, G.; Sironi, A.; D'Alfonso, G.; Romiti, P.; Freni, M. J. Organomet. Chem. 1983, 254, C37. (c) Beringhelli, T.; D'Alfonso, G.; Freni, M.; Ciana, G.; Moret, M.; Sironi, A. J. Chem. Soc., Dalton Trans. 1989, 1143. (d) Adams, R.D.; Falloon, S.B. J. Am. Chem. Soc. 1994, 116, 10540. (e) Adams, R.D.; Kwon, O.-S.; Perrin, J.L. J. Organomet. Chem. 2000, 596, 102.

2. Prest, D.W.; Mays, M.J.; Raithby, P.R.; Orpen, A.G. J. Chem. Soc., Dalton Trans. 1982, 737. (b) Prest, D.W.; Mays, M.J.; Orpen, A.G.; McMullan, R.K. J. Organomet. Chem. 1982, 240, 395.

3. For the structure of H3Re3(CO)9(triphos), see: Wang, S.R.; Wang, S.-L.; Cheng, C.P.; Yang, C.S. J. Organomet. Chem. 1992, 431, 215.

4. (a) Bott, S.G.; Shen, H.; Richmond, M.G. J. Organomet. Chem. 2004, 689, 3426. (b) Watson, W.H.; Kandala, S.; Richmond, M.G. J. Chem. Crystallogr. 2005, 35, 157. (c) Bott, S.G.; Shen, H.; Senter, R.A.; Richmond, M.G. Organometallics 2003, 22, 1953. (d) Watson, H.; Zhao, Y.; Richmond, M.G. J. Chem. Crystallogr. 2003, 33, 765.

5. Andrews, M.A.; Kirtley, S.W.; Kaesz, H.D. Inorg. Synth. 1975, 17, 66.

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