Raw clay material-based modified carbon paste electrodes for sensitive heavy metal detection in drinking water

Author:

Sanou Ali,Coulibaly Mariame,N’dri Seiny Roger,Tămaș Tudor Liviu,Bizo Liliana,Frentiu Tiberiu,Covaci Eniko,Abro Koutouan Désiré Martial,Dablé Pierre Jean-Marie Richard,Yao Kouassi Benjamin,Fort Carmen Ioana,Turdean Graziella LianaORCID

Abstract

AbstractA new electrode based on carbon paste (CP) modified with natural clay was used for heavy metals detection. The investigation of the raw clay material (X-ray diffraction, infrared spectroscopy, scanning electron microscopy, energy-dispersive X-ray spectroscopy, thermal analysis and particle size distribution) revealed different morpho-structural properties of the natural material. The electrochemical behaviour of the modified carbon paste electrode and its ability to detect heavy metals (Zn2+, Cd2+, and Cu2+) was studied by different electrochemical techniques like cyclic voltammetry (CV), electrochemical impedance spectroscopy (EIS), and square wave anodic stripping voltammetry (SWASV). Both electrochemical and analytical parameters of the investigated modified electrode recommend them as stable, sensitive and reproducible sensors for individual heavy metals detection.

Publisher

Springer Science and Business Media LLC

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