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Activation and Coupling

Published:1984 Issue: Volume: Page:87-150
ISSN:0341-2377
Container-title:Reactivity and Structure Concepts in Organic Chemistry
language:
Short-container-title:

Author:

Bodanszky Miklos,Bodanszky Agnes

Publisher

Springer Berlin Heidelberg

Link

http://link.springer.com/content/pdf/10.1007/978-3-642-96835-8_3

Reference125 articles.

1. Katsoyannis, P. G., du Vigneaud, V.: J. Amer. Chem. Soc. 76, 3114 (1954)

2. The acid chloride prepared from tosyl-L-isoleucine with thionyl chloride was obtained in crystalline form by extraction of the distillation residue with boiling hexane. On cooling rectangular tables separated melting at 54–56 °C. The crystalline material gave satisfactory N and Cl values on elemental analysis (Bodanszky, M., du Vigneaud, V.: J. Amer. Chem. Soc. 81, 2504 (1959)).

3. Swan, J. M., du Vigneaud, V.: J. Amer. Chem. Soc. 76, 3110 (1954)

4. Guttmann, S., Boissonnas, R. A.: Helv. Chim. Acta 43, 200 (1960)

5. Methanol is probably the solvent of choice for the hydrazinolysis of amino acid and peptide esters. If these are poorly soluble in methanol, hydrazinolysis can be attempted in suspension. Alternative solvents such as tetrahydrofurane, dio-xane or their mixtures with methanol are also useful. Hydrazine, however, reacts with ethyl acetate and, albeit slowly, with dimethylformamide as well. Dimethyl-formamide has often been used as solvent. In case of slow reactions addition of n-butanol might be helpful (Ferren, R. A., Miller, J. G., Day, A. R. : J. Amer. Chem. Soc. 79, 70 (1958)). Hydrazinolysis of s-benzyl-L-cysteine containing peptides could be performed advantageously in 2-methoxyethanol at 30 °C;

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1. Biochemical Methods;Chemistry of Plant Protection;1995

2. Antibodies in plant science;Acta Botanica Neerlandica;1991-03

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