Preparation of 2R, 3S, 2′R-nadolol enantiomer using S-(-)-menthyl chloroformate as a chiral derivatizing reagent-Reference-Cited by-同舟云学术

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Preparation of 2R, 3S, 2′R-nadolol enantiomer using S-(-)-menthyl chloroformate as a chiral derivatizing reagent

Published:2010-09 Issue:9 Volume:33 Page:1301-1306
ISSN:0253-6269
Container-title:Archives of Pharmacal Research
language:en
Short-container-title:Arch. Pharm. Res.

Author:

Sung Ju-Il,Van Thi Nguyen Ngoc,Park Min-Jung,Lee Seung-Beom,Lee Yong-Jae,Choi Seung-Ho,Kim Kyeong Ho

Publisher

Springer Science and Business Media LLC

Subject

Organic Chemistry,Drug Discovery,Molecular Medicine

Link

http://link.springer.com/content/pdf/10.1007/s12272-010-0902-1.pdf

Reference19 articles.

1. Aboul-Enein, H. Y. and Abou-Basha, L. I., HPLC Separation of nadolol and enantiomers on chiralcel OD column. J. Liq. Chromatogr. Relat. Technol., 19, 383–392 (1996).

2. Aboul-Enein, H. Y., High-performance liquid chromatographic enantioseparation of drugs containing multiple chiral centers on polysaccharide-type chiral stationary phases. J. Chromatogr. A, 906, 185–193 (2001).

3. Belas, F. J., Phillips, M. A., Srinivas, N. R., Barbhaiya, R. H., and Blair, I. A., Simultaneous determination of nadolol enantiomers in human plasma by high-performance liquid chromatography using fluorescence detection. Biomed. Chromatogr., 9, 140–145 (1995).

4. Bragg, W., Norton, D., and Shamsi, S. A., Optimized separation of β-blockers with multiple chiral centers using capillary electrochromatography-mass spectrometry. J. Chromatogr. B, 875, 304–316 (2008).

5. Dawson, B. A. and Black, D. B., Utilizing nuclear magnetic resonance (NMR) spectroscopy for assessing nadolol racemate composition. J.Pharm. Biomed. Anal., 13, 39–44 (1995).

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