Influence of curing duration and mixing techniques of bulk fill resin composites on bi-axial flexural strength and degree of conversion

Abstract

Objectives: The aim was to assess the influence of polymerization duration, method and resin manipulation techniques on the biaxial flexural strength (BFS) and degree of conversion (DC) of bulk fill resin composites (BFRC). Methods: One hundred and eighty disc specimens were fabricated using MultiCore (MC) and Core-It (CI) bulk fill resin composite. Each material group, specimens were divided into nine subgroups based on curing methods (Light cure for 10 and 20 s; and auto-cure) and mixing techniques (first auto-mix, second automix, and hand mix). BFS was tested with a ball indenter at a crosshead speed of 0.50 mm/min. DC was assessed for MC and CI materials for 10 s and 20 s light cure; and auto cure specimens using Fourier Transform-Infrared Spectroscopy (FTIR). Statistical data comparisons were performed using ANOVA, Bonferroni and Tukey-Kramer tests. Results: For MC and CI, BFS was highest in 10 s light cure specimens, however comparable to specimens cured for 20 s ( p > 0.05). Auto cure specimens showed lower BFS than light cured samples for both materials ( p < 0.05). Hand mixed specimens showed significantly compromised BFS compared to automix technique for MC and CI. DC % was comparable for 10 s and 20 s light cure methods for both materials ( p > 0.05), which was higher than DC % of auto cure bulk fill resins ( p < 0.05). CI showed higher DC % and BFS compared to MC bulk fill resin composite. Conclusion: Photo-polymerization duration of 10 and 20 s showed similar outcomes for BFS and DC %; and BFS for auto-mixed resins (MC and CI) was significantly higher than hand mixed resin. BFS and DC was higher in photopolymerized groups as compared to auto-cured resin regardless of the manipulation technique for both materials (MultiCore and Core it).