Effect of High Energy Ball Milling Washing Process on Properties of Nd<sub>2</sub>Fe<sub>14</sub>B Particles Obtained by Reduction-Diffusion-Reference-Cited by-同舟云学术

Effect of High Energy Ball Milling Washing Process on Properties of Nd₂Fe₁₄B Particles Obtained by Reduction-Diffusion

Published:2019-09 Issue: Volume:822 Page:244-251
ISSN:1662-9795
Container-title:Key Engineering Materials
language:
Short-container-title:KEM

Author:

Galkin Vitalii¹,Haider Kamran¹,Ahn Jong Bin¹,Kim Dong Soo¹

Affiliation:

1. Korea Institute of Geoscience and Mineral Resources

Abstract

Nd2Fe14B particles were obtained from mixture of neodymium oxide, iron oxide, boric acid and CaH2 by reduction-diffusion process. Two different washing processes were used for the separation of magnetic particles from Ca and CaO matrix: usual washing with water and planetary ball milling process in ethanol media. Nd2Fe14BHx hydrogenated state was formed after usual washing with water. Ethanol planetary ball milling washing procedure prevented the formation of Nd2Fe14B hydrides during washing. Variation of milling parameters allowed producing particles with different morphology such as spherical or flakes after planetary ball milling washing process. Influence of milling parameters on magnetic properties of Nd2Fe14B powder was investigated.

Publisher

Trans Tech Publications, Ltd.

Subject

Mechanical Engineering,Mechanics of Materials,General Materials Science

Link

https://www.scientific.net/KEM.822.244.pdf

Reference26 articles.

1. M. Sagawa, S. Fujimura, N. Togawa, H. Yamamoto, Y. Matsuura, New material for permanent magnets on a base of Nd and Fe (invited), Journal of Applied Physics. 55 (1984) 2083-2087.

2. D. Kim, E.S. Vasilieva, A.G. Nasibulin, D.W. Lee, O. V. Tolochko and B.K. Kim, Aerosol Synthesis and Growth Mechanism of Magnetic Iron Nanoparticles, Materials Science Forum 534-536 (2007) 9-12.

3. E.S. Vasil, O. V Tolochko, V.G. Semenov, V.S. Volodin and D. Kim, Mössbauer Spectroscopy Analysis of the Phase Composition of Iron-Based Nanoparticles, Technical Physics Letters 33 (2007) 40-43.

4. C.J. Choi, B.K. Kim, O. Tolochko and Li-Da, Preparation and characterization of magnetic Fe, Fe/C and Fe/N nanoparticles synthesized by chemical vapor condensation process, Reviews on Advanced Materials Science 5 (2003) 487-492.

5. N.O. Gonchukova, and T.V. Larionova, Effect of long-term annealing below the glass transition range on heat capacity and Curie temperature for metallic glasses, Fizika i Khimiya Stekla 20 (1994) 134-135.

Cited by 6 articles. 订阅此论文施引文献订阅此论文施引文献，注册后可以免费订阅5篇论文的施引文献，订阅后可以查看论文全部施引文献

1. Enhanced Nd-Rich Phase and Oxygen Control in Reduction-Diffusion Powders via Tailored Washing Process for Additive-Free Sintering of Fine Nd-Fe-B Particles;Journal of Magnetics;2024-03-31

2. Pelletizing highly porous covalent triazine framework under mild conditions and applying it as adsorbent for Ru3+ ions;Microporous and Mesoporous Materials;2024-02

3. Nd-Fe-B particles with reduced oxygen content and enhanced magnetic properties prepared through reduction-diffusion and novel washing process;Journal of Magnetism and Magnetic Materials;2023-07

4. Significance of Ionic Character Induced by Ga-Doped γ-Al2O3 on Polyethylene Degradation to the Precursors of Gasoline and Diesel Oil with a Trace Amount of Wax;Nanomaterials;2022-09-09

5. Synthesis of NdFeB Magnetic Particles With High (BH)_max From Their Optimized Oxide Powders Through Reduction–Diffusion Method;IEEE Magnetics Letters;2022