Geochemical investigation of alluvial sediments: validation of ICP-OES determination of heavy metals. A case study from the Utrata River Valley (central Poland)-Reference-Cited by-同舟云学术

Geochemical investigation of alluvial sediments: validation of ICP-OES determination of heavy metals. A case study from the Utrata River Valley (central Poland)

Published:2014-06-01 Issue:6 Volume:12 Page:687-699
ISSN:2391-5420
Container-title:Open Chemistry
language:
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Author:

Biro Miša¹,Kavšek Darja²,Karasiński Jakub³,Szwarczewski Piotr⁴,Bulska Ewa³,Vončina Darinka⁵

Affiliation:

1. 1CIVIS d.o.o.

2. 2Chemical-Technological Laboratory

3. 3Biological and Chemical Research Center

4. 4University of Warsaw

5. 5University of Maribor

Abstract

AbstractThe development and validation of a reliable analytical procedure for the determination of selected metals (Cd, Cr, Cu, Pb, Zn and Mn) in sediments accumulated in the Utrata River (Poland) is described. The aqua regia extraction followed by inductively coupled plasma optical emission spectrometry (ICP-OES) was used for this purpose. The optimized analytical procedure was validated, and adequate quality control actions were implemented in order to provide reliable data. The precision under’ within-laboratory’ reproducibility conditions was estimated from duplicate analysis. Certified reference material (CRM) was used in order to evaluate the accuracy of the results regarding the sewage sludge amended soil CRM 143R. The detection limits for all elements of interest were well-below their content in the investigated sediment samples. The obtained reliable data could be used for assessment of the relationship between human economic activity in the past and the geochemical features of the sediments.

Publisher

Walter de Gruyter GmbH

Subject

Materials Chemistry,General Chemistry

Link

http://link.springer.com/content/pdf/10.2478/s11532-014-0520-8.pdf

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