1-Aryl-3-nitro- and 3-Bromo-3-nitroprop-2-en-1-ones: Synthesis and Structural Features
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Published:2024-03
Issue:3
Volume:94
Page:497-507
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ISSN:1070-3632
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Container-title:Russian Journal of General Chemistry
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language:en
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Short-container-title:Russ J Gen Chem
Author:
Adyukov I. S., Pelipko V. V.ORCID, Baichurin R. I.ORCID, Litvinov I. A.ORCID, Makarenko S. V.ORCID
Abstract
Abstract
A method for producing a number of (E)-1-aryl-3-nitroprop-2-en-1-ones based on a synthetic condensation–dehydration strategy has been optimized. New (Z)-1-aryl-3-bromo-3-nitroprop-2-en-1-ones have been synthesised from (E)-1-aryl-3-nitroprop-2-en-1-ones using halogenation-dehydrohalogenation strategy to (E)-1-aryl-3-nitroprop-2-en-1-ones. The fine structure of nitro- and bromonitroenketones and it’s features were determined by 1H–1H NOESY NMR and X-ray diffraction analysis.
Publisher
Pleiades Publishing Ltd
Reference64 articles.
1. Sivanandan, S.T., Jesline, M.J., Nair, D.K., and Kumar, T., Asian J. Org. Chem., 2023, vol. 12, no. 1, art. e202200555. https://doi.org/10.1002/ajoc.202200555 2. Zou, D., Wang, W., Hu, Y., and Jia, T., Org. Biomol. Chem., 2023, vol. 21, no. 11, p. 2254. https://doi.org/10.1039/D3OB00064H 3. Parambil, S.P., Veettil, S.P., and Dehaen, W., Synthesis, 2021, vol. 54, no. 4, p. 910. https://doi.org/10.1055/a-1547-0196 4. Wu, J., Hu, F., Bai, G., Yang, Y., Bonne, D., Rodriguez, J., Yue, C., Wang, H., and Bao, X., Eur. J. Org. Chem., 2023, no. 26, art. e202300218. https://doi.org/10.1002/ejoc.202300218 5. Yuan, L., Kachalova, L., Khan, M.E., Ballini, R., Petrini, M., and Palmieri, A., J. Org. Chem., 2023, vol. 88, no. 7, p. 4770. https://doi.org/10.1021/acs.joc.2c02669
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