Toward a new lower limit for the minimum scattering vector on the very small angle neutron scattering spectrometer at Laboratoire Léon Brillouin

Author:

Brûlet Annie,Thévenot Vincent,Lairez Didier,Lecommandoux Sébastien,Agut Willy,Armes Steven P.,Du Jianzong,Désert Sylvain

Abstract

The main characteristics of the very small angle neutron scattering spectrometer (VSANS) under construction at the Laboratoire Léon Brillouin are a multibeam pinhole collimator converging onto an image plate detector. By combining tiny collimation (diaphragms of around 1 or 2 mm in diameter) with the small pixel size of the detector (0.15 × 0.15 mm), very high resolution measurements can be achieved. The resolution function of the instrument contains a contribution from gravity, which is reduced by the intermediate masks of the collimator. Owing to the relatively short length of the VSANS instrument (around 14 m), this effect remains weak, in good agreement with the predictions. With a prototype multibeam collimator, an incident wavelength of 0.9 nm and the detector located at 6 m from the sample, it is possible to accessqvalues as low as 4 × 10−3 nm−1with very highqresolution. Promising preliminary experiments with highqresolution are reported, which open up new fields to the SANS technique.

Publisher

International Union of Crystallography (IUCr)

Subject

General Biochemistry, Genetics and Molecular Biology

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