Crystal structure of 4,4′-(disulfanediyl)dipyridinium chloride triiodide-Reference-Cited by-同舟云学术

Crystal structure of 4,4′-(disulfanediyl)dipyridinium chloride triiodide

Published:2024-05-21 Issue:6 Volume:80 Page:641-644
ISSN:2056-9890
Container-title:Acta Crystallographica Section E Crystallographic Communications
language:
Short-container-title:Acta Crystallogr E Cryst Commun

Author:

Podda Enrico^ORCID,Aragoni M. Carla^ORCID,Caltagirone Claudia,De Filippo Greta,Garau Alessandra,Lippolis Vito^ORCID,Mancini Annalisa,Pintus Anna,Orton James B.,Coles Simon J.^ORCID,Arca Massimiliano^ORCID

Abstract

4,4′-(Disulfanediyl)dipyridinium chloride triiodide, C10H10N2S2 2+·Cl−·I3 −, (1) was synthesized by reaction of 4,4′-dipyridyldisulfide with ICl in a 1:1 molar ratio in dichloromethane solution. The structural characterization of 1 by SC-XRD analysis was supported by elemental analysis, FT–IR, and FT–Raman spectroscopic measurements.

Funder

Ministero per l'Ambiente e la Sicurezza Energetica

Fondazione di Sardegna

Engineering and Physical Sciences Research Council

Publisher

International Union of Crystallography (IUCr)

Link

https://journals.iucr.org/e/issues/2024/06/00/ee2006/ee2006.pdf

Reference40 articles.

1. Square-pyramidal bonding of I2 molecules at the I? nodes of a polyiodide infinite pseudo-cubic 3D-network

2. Reactions of Halogens/Interhalogens with Polypyridyl Substrates: The Case of 2,4,6‐Tris(2‐pyridyl)‐1,3,5‐triazine

3. Adducts of S/Se Donors with Dihalogens as a Source of Information for Categorizing the Halogen Bonding

4. An unprecedented non-classical polyinterhalogen anion made of [I₂Cl]⁻ and I₂ at the 2-(p-tolyl)selenopheno[2,3-b]pyridinium cation template

5. An Experimental and Theoretical Insight into I₂/Br₂ Oxidation of Bis(pyridin‐2‐yl)Diselane and Ditellane