1. Department of Analytical Chemistry, Faculty of Sciences, University of Granada, C/Fuentenueva s/n, E-18071 Granada, Spain, Department of Food Science, University of Bologna, Piazza Goidanich 60, I-47023 Cesena (FC), Italy, Department of food Science, University of Teramo,Via C. Lerici 1, I-64023 Mosciano Stazione (TE), Italy, and Department of Science, University of Pescara and Chieti, Viale Pindaro 42, I-65127 Pescara, Italy