PEEK Surface Treatment Using Nd: YAG, Riboflavin Activated by PDT, and Alumina Particles on Surface Roughness, Bond Failure, and Bond Integrity to Composite Resin

Abstract

Aims: Conditioning protocols, Airborne Particles of Alumina (ABP), Neodymium-Doped Yttrium Aluminium Garnet (Nd: YAG) laser, and Riboflavin (RF), were tested on PEEK disc bonded to composite restorations for surface roughness (Ra) and shear bond strength (SBS). Method and Material: Random sampling was used to divide 80 PEEK discs into four groups for surface conditioning. (n = 20). Group 1: Sulfuric acid (SA); Group 2: PDT (RF); Group 3: Alumina particle ABP; Group 4: NYL. Pretreated PEEK discs were measured for Ra using a surface profilometer. They were luted and bonded to composite resin discs. On Universal testing equipment, SBS was tested. Stereomicroscopes analyzed failure type. Data was analyzed using one-way ANOVA and Tukey’s test. Results: The SA-treated group had the highest Ra (1.411 ±0.043 μm). However, PDT (RF) treated tissues had the lowest mean Ra score (1.299 ± 0.019 μm). Regarding SBS, the SA-treated group (11.83±0.82 MPa) had the highest mean score. PDT (RF) (10.23±0.64 MPa) treated specimens showed the lowest bond integrity values. The most common fracture type in all investigated groups is cohesive failure. Conclusion: Airborne alumina, riboflavin, and Nd: YAG laser could replace PEEK sulfuric acid to improve composite cement bond integrity and surface roughness.