Characterization of graphene nanosheets obtained by a modified Hummer's method

Author:

Hack Renata1,Correia Cláudia Hack Gumz2,Zanon Ricardo Antônio de Simone1,Pezzin Sérgio Henrique1

Affiliation:

1. Universidade do Estado de Santa Catarina, Brazil

2. Universidade da Região de Joinville, Brazil

Abstract

ABSTRACT Natural graphite is an inexpensive and abundant source to obtain graphene nanosheets. The most efficient method for large-scale production is the chemical method, which is based on the oxidation of natural graphite. This paper reports the synthesis and characterization of graphene obtained by the Hummers method with some modifications. The results indicate a high degree of graphite oxidation, proving that the process was efficient. Analyses of field emission scanning electron microscopy (FEG), transmission electron microscopy (TEM), Raman spectroscopy, thermogravimetric analysis (TGA) and X-ray diffraction showed that the graphene produced presented characteristics similar to the commercial graphene.

Publisher

FapUNIFESP (SciELO)

Subject

General Physics and Astronomy,General Materials Science,General Chemistry

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