CdS-silica xerogel nanocomposites: Processing-induced textural changes

Author:

Blanco E.,Litrán R.,Ramírez-del-Solar M.,de la Rosa-Fox N.,Esquivias L.

Abstract

CdS-silica xerogel composites were prepared from tetramethoxysilane, acidic water, and formamide mixtures homogenized by high power ultrasounds. Different concentrations of Cd(NO3)2 were added. CdS semiconductor nanoparticles were precipitated by H2S gas diffusion through the sonogel porous structure. Composite mechanical properties were enhanced by an impregnation process by the gel soaking in the same sol as-prepared. Textural parameters evolution is compared to the salt content in order to find the best performance to CdS nanocrystal growth. The impregnation process allows a better composite protection.

Publisher

Springer Science and Business Media LLC

Subject

Mechanical Engineering,Mechanics of Materials,Condensed Matter Physics,General Materials Science

Cited by 11 articles. 订阅此论文施引文献 订阅此论文施引文献,注册后可以免费订阅5篇论文的施引文献,订阅后可以查看论文全部施引文献

1. Influence of processing induced textural effect on aggregation level in CuPc?SiO2 sonogel composites;Journal of Non-Crystalline Solids;2003-04

2. Sol-gel Processing;Handbook of Nanophase and Nanostructured Materials;2003

3. Nanocomposites prepared by sol-gel methods;Nanostructured Materials and Nanotechnology;2002

4. Sonogels and derived materials;Applied Organometallic Chemistry;1999-05

5. Formation of LaF3 microcrystals in sol–gel silica;Journal of Non-Crystalline Solids;1999-03

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