Coatings Prepared by Electro-Spark Alloying with SHS Electrode Materials Based on Ti-B-Fe-AlN

Author:

Bolotskaia Anastasia1ORCID,Avdeeva Varvara2ORCID,Bazhin Pavel1ORCID,Mikheev Maksim1ORCID,Stolin Alexander1,Novikov Vseslav3ORCID,Kovaleva Marina3ORCID,Sirota Viacheslav4

Affiliation:

1. Merzhanov Institute of Structural Macrokinetics and Materials Sciences, Russian Academy of Sciences, Akademika Osipyana 8, 142432 Chernogolovka, Russia

2. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii Prospekt 31, 119991 Moscow, Russia

3. Joint Research Center of Belgorod State National Research University “Technology and Materials”, Research Institute of Materials Science and Innovative Technology, Belgorod State National Research University, Pobeda 85, 308015 Belgorod, Russia

4. Science and Innovation Department, Center for High Technologies of the Belgorod State Technological University, Belgorod State Technological University Named after V.G. Shoukhov, Kostyukov 46, 308012 Belgorod, Russia

Abstract

In this work, the features of the phase composition, structures, and properties of coatings obtained on a high-speed steel substrate (steel R6M5) were studied. The coatings were prepared using the ESA method (electro-spark alloying). Electrode materials prepared through self-propagating high-temperature synthesis (SHS) based on (Ti-B-Fe)xAlN with the addition of nanosized AlN particles in the amount of x = 0.5, 10, 15 wt % were used as electrodes. The structure, phase composition, and physical and mechanical properties of the SHS electrode materials are reported. It was found that the coatings inherited the structure of the SHS electrode material and formed two characteristic zones for x = 0 and three zones for x = 5, 10, 15. The surface hardness of the substrate made of the high-speed steel R6M5 with the developed coatings was found to increase up to five times compared to the uncoated substrate. It was found that the wear resistance of the samples with the coating was four to six times higher than that of uncoated samples.

Funder

Ministry of Science and Higher Education of the Russian Federation

Publisher

MDPI AG

Subject

Materials Chemistry,Surfaces, Coatings and Films,Surfaces and Interfaces

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