Validation of a Headspace Gas Chromatography with Flame Ionization Detection Method to Quantify Blood Alcohol Concentration (BAC) for Forensic Practice

Author:

Cerioni Alice1ORCID,Mietti Gianmario1ORCID,Cippitelli Marta1ORCID,Ricchezze Giulia1ORCID,Buratti Erika1ORCID,Froldi Rino1,Cingolani Mariano1ORCID,Scendoni Roberto1ORCID

Affiliation:

1. Forensic Medicine Laboratory, Institute of Legal Medicine, University of Macerata, 62100 Macerata, Italy

Abstract

Alcohol consumption is a major social and forensic issue. It is often the cause of road accidents, industrial accidents, suicides and other crimes. On account of this, it is of fundamental importance in forensic toxicology to correctly quantify blood alcohol concentration (BAC). In this work, a straightforward method for the quantification of ethanol from blood samples by means of headspace gas chromatography with flame ionization detection is presented and validated. For method validation linearity, limit of detection (LOD), lower limit of quantification (LLOQ), accuracy, precision (% CV) and interference studies were carried out. All the validation conditions were satisfied according to the acceptance criteria. Proof of applicability was performed on 50 real blood samples, showing that the method was effective.

Funder

European Union–NextGenerationEU under the Italian Ministry of University and Research (MUR) National Innovation Ecosystem

Publisher

MDPI AG

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