Efficiency Dependence of Radiation-Assisted Ceramic Synthesis Based on Metal Oxides and Fluorides on Initial Powder Particle Sizes

Author:

Lisitsyn Victor1ORCID,Polisadova Elena1,Lisitsyna Liudmila2,Tulegenova Aida34ORCID,Denisov Igor1,Golkovski Mikhail5

Affiliation:

1. Department of Materials Science, Engineering School, National Research Tomsk Polytechnic University, 30, Lenin Ave., Tomsk 634050, Russia

2. Department of Physics, Chemistry and Theoretical Mechanics, Tomsk State University of Architecture and Building, 2, Solyanaya Sq., Tomsk 634003, Russia

3. Institute of Applied Science & Information Technology, 280, Baizakov Str., Almaty 050042, Kazakhstan

4. National Nanotechnology Laboratory of Open Type (NNLOT), Al-Farabi Kazakh National University, 71, Al-Farabi Ave., Almaty 050040, Kazakhstan

5. Budker Institute of Nuclear Physics, SB RAS, 11, Lavrentiev Ave., Novosibirsk 630090, Russia

Abstract

The study is devoted to investigating the efficiency dependence of radiation-assisted ceramic synthesis based on metal oxides and fluorides on initial powder particle sizes. The synthesis was performed for 30 series of ceramic samples, including MgO, Al2O3, ZnO, ZrO2, MgF2, and complex compositions: cerium-activated yttrium-aluminum garnet (Y3Al5O12), spinel AlMgO4, and tungstate MgWO4. The synthesis efficiency was evaluated on the mixture weight magnitude losses, morphology, and relative weight of the obtained ceramic samples. Based on the analysis of the synthesis results and measuring the particle distribution spectra of the initial materials, the criteria for selecting the initial materials were established, and possible explanations for the correlation between synthesis efficiency and the initial materials morphology were proposed.

Funder

Russian Science Foundation of the Russian Federation

Publisher

MDPI AG

Subject

Radiology, Nuclear Medicine and imaging,Instrumentation,Atomic and Molecular Physics, and Optics

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