Microstructure and Fracture Toughness of Fe–Nb Dissimilar Welded Joints

Abstract

The relation between the microstructure and mechanical properties of the Fe–Nb dissimilar joint were investigated using nanoindentation. The weld metal consists mainly of Fe2Nb, α-Fe + Fe2Nb, Nb (s,s) and Fe7Nb6 phases. Radial cracks initiate from the corners of the impressions on the Fe2Nb phase (~20.5 GPa) when subjected to a peak load of 300 mN, whereas the fine lamellar structures (α-Fe + Fe2Nb) with an average hardness of 6.5 GPa are free from cracks. The calculated fracture toughness of the Fe2Nb intermetallics is 1.41 ± 0.53 MPam1/2. A simplified scenario of weld formation together with the thermal cycle is proposed to elaborate the way local phase determined the mechanical properties.