Production of Synthetic Carbonate Rocks Using Limestone Mining Waste: Mineralogical, Petrophysical and Geomechanical Characterization

Author:

dos Santos Yago Ryan Pinheiro1ORCID,Gomes Igor1ORCID,Lima Analice1,Barbosa José1ORCID,Correia Filho Osvaldo1,Antonino Antonio Celso Dantas1ORCID,Duarte Daniel1,Rodrigues Marcos2ORCID

Affiliation:

1. Centre for Technology and Geosciences, Department of Civil Engineering, Federal University of Pernambuco, 100 Arquitetura Ave., Recife 50670-901, Brazil

2. Centre for Exact Sciences, Department of Petroleum Engineering, Federal University of Rio Grande do Norte, Natal 59078-970, Brazil

Abstract

Carbonate rocks are important for the petroleum industry, as they contribute significantly to hydrocarbon reserves, although their analysis is complex due to the high cost of core sampling and their high heterogeneity; for this, synthetic rocks aim to provide relatively homogeneous samples with analogous characteristics to natural rocks. In this research, synthetic carbonate rocks were produced by mixing a fixed ratio between limestone powder, obtained from limestone mining waste, and epoxy resin as a cementing material, using compaction energy for consolidation. The work aimed to produce homogeneous samples with high strength, reproducing the intergranular pore system for future applications in rock–fluid interaction analysis. The characteristics and structure of the samples were investigated through X-ray computed microtomography, petrographic images, petrophysical, chemical and geomechanical tests. Results showed a direct increasing relationship between porosity and permeability and a tendency for mechanical strength (UCS) to decrease with increasing porosity. When compared with the natural carbonate rocks, these presented similarities in their mechanical properties and petrophysical measurements, showing that the methodology can be considered as an alternative for the obtention of a realistic material that can be used for future experiments regarding rock mechanics and rock–fluid interaction for prediction of carbonate rocks’ behavior.

Funder

PETROBRAS, National Council for Scientific and Technological Development-CNPq and Energi Simulation

Publisher

MDPI AG

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