Visible‐Light Induced C‐3 Carbamoylation of Quinoxalinones Assisted by EDA Complex

Author:

Azim Aznur1,Mandal Tanumoy1,Vasudevan Vidhul1,Patra Shefali1,De Sarkar Suman1

Affiliation:

1. Department of Chemical Sciences Indian Institute of Science Education and Research Kolkata Mohanpur 741246 West Bengal India

Abstract

AbstractA visible‐light‐promoted strategy for the decarboxylative C‐3 carbamoylation of quinoxalinone scaffolds is developed. This approach initiates through the formation of an EDA complex between oxamic acid and quinoxalinone. Successive SET and decarboxylative carbamoylation construct the C−C bond. This method utilizes aerial oxygen as the green oxidant and eradicates the process from the use of external photocatalysts and transition metals. Detailed synthetic and photophysical studies enlighten the reaction pathway.

Funder

Indian Institute of Science Education and Research Kolkata

Publisher

Wiley

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