Optimization in the reprocessing of recycled polyamide 6 reinforced with 30 wt% Glass Fiber (PA6/GF30) using mixture design

Author:

Haddar Manel12ORCID,Koubaa Sana2,Issaoui Maryam2,Frikha Ahmed3

Affiliation:

1. National Engineering School of Sfax (ENIS), University of Sfax Sfax Tunisia

2. Laboratory of Applied Fluids Mechanics of Process Engineering and Environment National Engineering School of Sfax (ENIS), University of Sfax Sfax Tunisia

3. Electro‐Mechanical Systems Laboratory (LASEM) National Engineering School of Sfax (ENIS), University of Sfax Sfax Tunisia

Abstract

AbstractIn the present study, polyamide 6 reinforced with 30 wt% Glass fiber (PA6/GF30) used in automotive industry was reprocessed via injection molding. The virgin and recycled PA6/GF30 samples were characterized by chemical, rheological, mechanical, and morphological properties as a function of the number of processing cycles. After each reprocessing cycle, a decrement in mechanical properties in tensile, bending, and impact strength was revealed for different combination of cycle number (N0 [for the virgin PA6/GF30], N1 [for the first recycled PA6/GF30], N2 [for the second recycled PA6/GF30], and N3 [third recycled PA6/GF30 sample]) in the composite mixture. A simplex‐centroid mixture design (SCMD) was used to evaluate the effect of combining Ni (i=0,1,2) on the mechanical properties of composite samples for optimization. Graphical comparison of experimental results using regression models showed a high degree of correlation. Results revealed that the ternary N0N1N2 blends composite made up of 67.97 wt% N0, 23.13 wt% N1, and 8.89 wt% N2 exhibited the best mechanical properties. Furthermore, a good correlation between the scanning electron microscopy (SEM) observations and tensile test results was observed. Hence, the new reprocessed formulation presents a cost‐effective alternative of virgin PA6/GF30 for different engineering applications.

Publisher

Wiley

Subject

Polymers and Plastics

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