Coupling effect of non‐relaxing and high temperature on fatigue properties of carbon‐black filled isoprene rubber

Author:

Luo Ganfang12ORCID,Song Ziwei3,Guo Jialin3,Zhang Chi13ORCID,Yang Xiaoniu123ORCID

Affiliation:

1. State Key Laboratory of Polymer Physics and Chemistry, Changchun Institute of Applied Chemistry Chinese Academy of Sciences Changchun People's Republic of China

2. School of Applied Chemistry and Engineering University of Science and Technology of China Hefei People's Republic of China

3. Lab of Polymer Composites Engineering, Changchun Institute of Applied Chemistry Chinese Academy of Sciences Changchun People's Republic of China

Abstract

AbstractThis paper presents an extensive experimental investigation on fatigue properties of carbon‐black filled isoprene rubber under complex loadings. A basic life prediction model taking strain energy density as fatigue parameter is first proposed based on fatigue crack growth tests and uniaxial tension fatigue tests under relaxing loads at room temperature. A database of fatigue life including relaxing and non‐relaxing is established through a great number of fatigue tests under five temperatures. Based on the database, two empirical parameters, that is, temperature factor (NRT/NHT) and life reinforcement factor (Re), are introduced to quantitatively characterize the coupling effects of high temperature and non‐relaxing loads on fatigue life. The fatigue mechanisms under different conditions are compared via wide‐angle x‐ray diffraction tests and postmortem analysis. It reveals that the weakening of life reinforcement at high temperatures is closely related to the strain induced crystallization behavior of rubber.

Funder

National Natural Science Foundation of China

Publisher

Wiley

Subject

Materials Chemistry,Polymers and Plastics,Surfaces, Coatings and Films,General Chemistry

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