Atomic resolution imaging using a novel, compact and stiff scanning tunnelling microscope in cryogen‐free superconducting magnet

Author:

Esmaeilzadeh Behnam12ORCID,Touqeer Muhammad12,Junwei Liu12,Zheng Shaofeng12,Geng Tao12,Hou Yubin13,Lu Qingyou1234

Affiliation:

1. High Magnetic Field Laboratory Hefei Institutes of Physical Science Chinese Academy of Sciences Hefei Anhui China

2. Hefei National Research Center for Physical Sciences at the Microscale University of Science and Technology of China Hefei Anhui China

3. Anhui Key Laboratory of Low‐Energy Quantum Materials and Devices, High Magnetic Field Laboratory, HFIPS Chinese Academy of Sciences Hefei Anhui China

4. Anhui Laboratory of Advanced Photon Science and Technology University of Science and Technology of China Hefei Anhui China

Abstract

AbstractWe present the design and performance of a novel scanning tunnelling microscope (STM) operating in a cryogen‐free superconducting magnet. Our home‐built STM head is compact (51.5 mm long and 20 mm in diameter) and has a single arm that provides complete openness in the scanning area between the tip and sample. The STM head consists of two piezoelectric tubes (PTs), a piezoelectric scanning tube (PST) mounted on a well‐polished zirconia shaft, and a large PT housed in a sapphire tube called the motor tube. The main body of the STM head is made of tantalum. In this design, we fixed the sapphire tube to the frame with screws so that the tube's position can be changed quickly. To analyse the stiffness of the STM head unit, we identified the lowest eigenfrequencies with 3 and 4 kHz in the bending modes, 8 kHz in a torsional mode, and 9 kHz in a longitudinal mode by finite element analysis, and also measured the low drift rates in the XY plane and in the Z direction. The high performance of the home‐built STM was demonstrated by images of the hexagonal graphite lattice at 300 K and in a sweeping magnetic field from 0 T to 9 T. Our results confirm the high stability, vibration resistance, insensitivity to high magnetic fields and the application potential of our newly developed STM for the investigation of low‐frequency systems with high static support stiffness in physics, chemistry, material and biological sciences.

Funder

National Key Research and Development Program of China

National Natural Science Foundation of China

Publisher

Wiley

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