Mn‐doped Pb(In1/2Nb1/2)O3‐Pb(Sc1/2Nb1/2)O3‐PbTiO3 relaxor ferroelectric ceramics for high‐power piezoelectric applications

Author:

Zhao Weijia1,Yang Shuai1,Wang Chao1ORCID,Wang Mingwen1,Gao Xiangyu1,Li Jinglei1,Li Fei1ORCID

Affiliation:

1. Electronic Materials Research Laboratory (Key Lab of Education Ministry), State Key Laboratory for Mechanical Behavior of Materials and School of Electronic Science and Engineering Xi'an Jiaotong University Xi'an China

Abstract

AbstractAchieving comprehensive improvement in both piezoelectric coefficient (d33) and mechanical quality factor (Qm) has become a key issue in the research of high‐power piezoelectric ceramics. Here, we focused on Mn‐doped Pb(In1/2Nb1/2)O3‐Pb(Sc1/2Nb1/2)O3‐PbTiO3 (PIN‐PSN‐PT) relaxor ferroelectric ceramics, where Mn‐doping is employed to enhance Qm. The effects of doping concentration and PT content on phase structure, ferroelectric, dielectric, and electromechanical properties were systematically studied. The well radius matching between Mn ions and B‐site ions facilitates the ion substitution and significantly increases the concentration of oxygen vacancies, thereby enhancing the domain wall pinning effect. A significantly weakened mutual constraint relationship between d33 and Qm is observed in the 2 mol% Mn‐doped PIN‐PSN‐PT ceramics with tetragonal phase, which exhibits Qm exceeding 3000 while maintaining d33 higher than 320 pC/N and Curie temperature higher than 300°C, leading to the vibration velocity over 1.15 m/s. Rayleigh analysis reveals the higher intrinsic piezoelectric response in high PT components compared to that in low PT components, which was thought to be the origin for the weakened mutual constraint relationship between d33 and Qm in tetragonal Mn‐doped PIN‐PSN‐PT ceramics.

Funder

National Natural Science Foundation of China

China Postdoctoral Science Foundation

Publisher

Wiley

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