Author:
Hamada Tatsuo,Kobayashi Yukinari
Subject
Organic Chemistry,Drug Discovery,Biochemistry
Reference13 articles.
1. The first stereoselective total synthesis of lankanolide. Part 1: Computer-assisted design and lactonization of model seco-acid derivatives
2. Convenient general method for the preparation of primary alkyllithiums by lithium-iodine exchange
3. Keck, G. E.; Abott, D. E. Tetrahedron Lett. 1984, 25, 1883. In this case, the ratio of desired anti-Cram syn-adduct to undesired products was 6:1, although the structures of the undesired products were not determined.
4. 3-Methoxybenzyl (3-MPM) and 3,5-dimethoxybenzyl (3,5-DMPM) protecting groups for the hydroxy function less readily removable than 4-methoxybenzyl (MPM) and 3,4-dimethoxybenzyl (DMPM) protecting groups by DDQ oxidation.
5. Yamamoto, Y.; Yatagai, H.; Ishihara, Y.; Maeda, N.; Maruyama, K. Tetrahedron 1984, 40, 2239 and reference cited therein. In our case, the ratio of Cram to anti-Cram was 5:1, although only erythro-type adduct was obtained.
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