Author:
Ewbank Paul C,Nuding Guido,Suenaga Hikaru,McCullough Richard D,Shinkai Seiji
Subject
Organic Chemistry,Drug Discovery,Biochemistry
Reference10 articles.
1. Self-Assembly and Disassembly of Regioregular, Water Soluble Polythiophenes: Chemoselective Ionchromatic Sensing in Water
2. For a review of regioregular polythiophene synthesis and properties, see: McCullough, R. D.; Ewbank, P. C. In Handbook of Conducting Polymers, 2nd ed.; Skotheim, T. A.; Elsenbaumer, R. L.; Reynolds, J. R., Eds.; Marcel Dekker: New York, 1998; p. 225.
3. For a review of conformation related chromatism, see: LeClerc, M.; Faı̈d, K. ibid. 695.
4. Designing conducting polymer-based sensors: selective ionochromic response in crown ether-containing polythiophenes
5. Synthesis of 2-chlorotetrahydropyran (THP-Cl): A sample of 3,4-dihydro-2-H-pyran (10 mL, 190.6 mmol) was dissolved in anhydrous Et2O and cooled in an ice bath. A 1.0 M solution of HCl in Et2O (Aldrich; 130 mmol) was added dropwise, and the reaction was stirred for 3 h. Concentration and distillation (46°C, 0.16 T) afforded a colorless oil (6.8 g, 56 mmol, 51% yield). This is a simplification of the procedure first reported by: Eliel, E. L.; Daignault, R. A. J. Org. Chem. 1965, 30, 2450.
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